Particulate Systems

DVS Advantage (Dynamic Vapor Sorption)


DVS Advantage

 

DVS Advantage, Dynamic Vapor Sorption (DVS) is the world leading gravimetric technique for studying water and organic sorption/adsorption on particulate materials. Invented by Surface Measurement Systems (SMS) in 1994, DVS revolutionized the field of gravimetric moisture sorption measurement, replacing outdated, time and labor intensive desiccators methods with intelligent computer based instrumentation; both orders of magnitude faster and more accurate than desiccator methods. The DVS family of instruments are designed, developed and produced by SMS and all include the SMS UltraBalance at the heart of the system. DVS instruments are now used in 100’s of laboratories throughout the world, in a wide range of research as well as QA applications supporting problems in formulation, product stability, moisture uptake, packaging and product development for solid state materials. For more information, or to discuss any particular requirement, please contact us via DVSinfo@micromeritics.com

 


DVS Advantage combines the best in microbalance, gas flow and vapor measurement technologies to deliver unsurpassed performance in terms of experimental design as well as instrument accuracy and repeatability.

The Advantage uses a dry carrier gas, usually nitrogen, and the user can select one of any two vapor sources. Precise control of the ratio of saturated and dry carrier gas flows is enabled with mass flow control combined with the use of unique real time vapor concentration monitoring for both water and organics. A known concentration of the selected vapor then flows over a sample suspended from a recording ultra-microbalance, which measures the weight change caused by sorption or desorption of the vapor molecule. It is these dynamic flow conditions that enable the sorption/desorption process to be so rapidly studied.

The sample may be pre-heated if desired as a further experimental option, and which in some cases may speed up the analysis cycle time as in the case of bulk absorption or the drying of inorganic hydrates. This heating can be as a single step, or at a controlled ramp rate of temperature.

The temperature of the whole system is user selectable and precisely controlled under closed loop conditions to ensure that the solute vapor pressure at the sample is constant. Isolation valves at the solvent reservoirs ensure there is no solute contamination of the sample area when p/pº of zero is requested, ensuring that a true p/pº zero is always obtained.

The incredible sensitivity and precision of DVS Advantage enables the use of very small samples (typically 1 – 30mg) thus allowing equilibrium to be reached even more quickly.

Safety being paramount, there is a fully automated inert gas purge facility, and organic leak sensor system shut down interlock in the case of accidental organic vapor release. The instrument is fully programmable and controlled by DVS Advantage software through a smart operator interface that meets the highest standards of data integrity and security.

A full suite of data analysis modules running under Excel® allow one-click calculations and reports to be generated.

Features and Benefits:

  • Single finger access for fast sample loading.
  • High performance digital microbalance.
  • Pre-heating of the sample up to 200ºC.
  • Full digital control of sample pre-heater and analysis temperatures.
  • Multiple vapor reservoirs for rapid change from water to organic solutes.
  • Multi-component vapor capability option.
  • Unique in line transducer technology for measuring real time organic or water vapor concentrations.
  • Compatible with NIR and Raman fibre optic systems.
  • DVS Color Video option with full data annotation of digital images.
  • Full automation of the widest range of experimental methods.
  • Smart Windows XP operator interface with full 21CFR part 11 compliance.
  • Comprehensive data analysis macros and advanced macros with 21CFR part 11 compliance.
  • Optional comprehensive extended Isotherm analysis software.
  • Dedicated worldwide applications and technical support.

Examples of DVS Applications:

  • Moisture uptake behavior of food and natural materials.
  • Stability and caking of food ingredients.
  • Moisture diffusion into blister packaging systems.
  • Moisture sorption of hydrophobic pharmaceutical materials.
  • Surface energies and surface areas of powders using organic vapor probes.
  • Determination of deliquescence points.
  • Moisture-induced glass transition in an amorphous material.
  • Determination of amorphous contents.
  • Pharmaceutical stability, drying and thermal degradation.
  • Adsorption of porous materials.

Product Information : Dynamic Vapor Sorption Archived Webinar


 Contact Information:

Patrick Wommack
General Manager
Office: 770.662.3681
Cell: 404.229.8384
email:
pat.wommack@micromeritics.com
Mike Still
Product Support Manager
Office: 770.662.3651
email:
mike.still@micromeritics.com
U.S. Sales:
770.662.3633
email:
ussales@micromeritics.com